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http://hdl.handle.net/2289/5590
Title: | Synthesis and characterisation of novel alkoxycyanobiphenyl-substituted rufigallols |
Authors: | Pal, Santanu Kumar Kumar, Sandeep |
Keywords: | cyanobiphenyl, oligomer disc–rod hybrids microwave-assisted synthesis |
Issue Date: | Feb-2013 |
Publisher: | Taylor & Francis |
Citation: | Liquid Crystals, 2013, Vol. 40, p281-292 |
Abstract: | Microwave-assisted synthesis of novel alkoxycyanobiphenyl-substituted rufigallols are reported by systematically replacing one, two, four, five or six cyanobiphenyl-tethered alkoxy chains. The synthesis of the target compounds was challenging since classical reactions failed to produce these hybrids. Chemical structures of the hybrids were determined by 1H nuclear magnetic resonance (NMR), 13C NMR, infrared, ultraviolet spectroscopy and elemental analysis. The thermotropic liquid crystalline properties of the new compounds were investigated by polarising optical microscopy, differential scanning calorimetry and X-ray diffractometry |
Description: | Restricted Access. |
URI: | http://hdl.handle.net/2289/5590 |
ISSN: | 0267-8292 1366-5855 (Online) |
Alternative Location: | http://dx.doi.org/10.1080/02678292.2012.747112 |
Copyright: | 2013 Taylor & Francis |
Appears in Collections: | Research Papers (SCM) |
Files in This Item:
File | Description | Size | Format | |
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2013_LC_40_281.pdf Restricted Access | Restricted Access | 996.57 kB | Adobe PDF | View/Open Request a copy |
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